Merck Expert: 5 Tips for Qualifying Pallet-Sized Thermal Shippers

At the ISTA Forum’s TempPack in Houston (May possibly 1-3, 2023), Lee Menszak, associate director, engineering at Merck, shared strategies and concerns for qualifying pallet-sized shippers, wherever the risk is frequently much higher than that of a compact parcel-sized shipper.

“Large shippers are various than compact shippers for a range of causes. The kinds that I would level out the most are that the payloads are more substantial, they are highly-priced, and they would be tough and time-consuming to exchange. So it is really crucial that you get it proper the initially time, and that you have a sturdy resolution,” reported Menszak.

He also highlighted that substantial shippers have extended pack-out durations, much larger temperature gradients within the payload house, and a higher selection of closure points in the course of assembly, amid other factors.

1. Will not disregard regional person requirements (together with security)

Menszak showed attendees a photograph in which an operator is within the shipper loading dry ice even though donning a complete backpack respirator. “The purpose is in the Netherlands, it is a need you ought to do this. You will need to know the particulars of the particular person state. Do not imagine about your viewpoint from your desk when you are qualifying the shipper,” he mentioned, introducing that you have to take into account basic safety for the duration of loading, as dry ice is controlled as a risky good. IATA PI 954 calls for precise labeling and sufficient ventilation so that tension make-up isn’t going to rupture the packaging.


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2. Thou shalt know thy shipper 

“My quantity a person rule of qualification is ‘Thou shalt know thy shipper,’” he stated. “When you get accomplished with the qualification, you really should know it as perfectly as—or better—than the maker, you need to come to be the SME. The previously you do it the much better.”

If the room for dry ice in the shipper is 2.75 inches, you just cannot load a 3.5-inch block of dry ice. If the dry ice block is 1.5 inches, it will rattle and won’t fill the room. He extra, “My problem to you is what excellent is qualification if when you give it to a consumer web page, the dry ice they have offered isn’t going to perform?”

3. TOCS is a person necessity 

Time out of controlled storage (TOCS) is the time to go from wherever the solution is stored to exactly where it is packed out. Prior to the pack out, it’s envisioned to have a delay whilst planning the payload for loading, with time for top quality checks, securing the payload on to the pallet with banding or strapping, and other regimen operational handling prerequisites.

TOCS must be controlled and minimized, but it also demands to be quantified and be consultant of what is wanted. “It is for the user to determine, so you have to have to chat to those people liable for carrying out the packout,” he observed.

Menszak mentioned he has uncovered TOCS is generally 30 minutes but encountered a single web site that wanted just one hour from removing from -40°C to the shipper door close. This person prerequisite specification requires to be bundled in the qualification testing, so it’s essential to permit your qualification lab know.


Max Load and Worst Case

“What’s the worst scenario? In my experience—not to be taken as law—max load, max mass is the worst situation. I have found it the reverse way wherever dry ice sublimates, CO2 gas sinks, and the hot air rises. As opposed to compact shippers, convection dominates here [in pallet-sized shippers]. You need to take a look at to obtain out what your worst-scenario scenario is.”

Lee Menszak


4. Rationale is a neglected spot

As he defined, “It’s one thing to say that you’re heading to use this profile or this configuration, but the rationalities need to be involved. Why? For the benefit of the approvers, they need to have to fully grasp why you might be performing what you’re carrying out. There’s a far better explanation, nevertheless, to be truthful. Two, 3 years down the highway when you get audited on the shippers you may well have overlooked.”

Also, it might be another person presenting your protocol who is in the dim about why you did what you did. Documenting the rationale will make clear why you made these choices—whether it is you or a different human being in the audit.

Some parameters may be apparent for inclusion in your rationale these kinds of as ambient profile, duration, payload and thermal mass, and refrigerant loading. But there are other actions to take into consideration, which could really precede qualification this sort of as CO2 sensitivity, cyro temperature tolerance, container closure integrity, and re-icing. “Dry ice sublimates… CO2 gas would not know it is not allowed to interact with the product. If you’re applying dry ice, you will need to have a CO2 sensitivity test in progress of qualification concluding that CO2 ingress is not an difficulty with your solution,” Menszak explained. Additionally, plastics, tubing, and clamps can be delicate to cracking at lower temperatures, so screening main packaging early on is crucial.

5. Shipper to shipper variation

Although it is not a prerequisite, Menszak highly advocates you take a look at shipper-to-shipper variability. If you fly a fleet of a dozen hardshell shippers, how do you know that they are all executing similarly? 

Though the seller supplies an examination, the only way to come across out is to essentially test. “And it’s a basic examination. Load them up with dry ice, set the temperature screens in at bare minimum load, and you allow them run. It does not have to have a laboratory it can be in the warehouse. At the stop of testing, you may, as I have, come across just one which is an underperformer. So from Day A single, you have a troublesome shipper. Here is your justification. Go back to the seller and say this one’s poor, we will need a replacement. And they also know they improved give you a fantastic one back because you are going to exam it to find out,” he claimed.

He stated there is a further good explanation for carrying out this examination: when a long time go by, suddenly you get a shipment that failed to go as expected, without having a excellent rationalization. “You can repeat this exam. So you can test shipper #4 which is a problem now and evaluate the benefits and how it executed when it was brand new,” Menszak said. “There may well be degradation. What is the lifestyle expectancy of the shipper? My expertise is that the manufacturers will give you a vague reply due to the fact it is dependent on the usage, the range of turns. So it is a great way, five decades down the road to say, ‘We’re setting up to see some difficulties. Let’s run by the exact test we did when they have been new and see what is heading on.’” This can enable you figure out if you’ll will need to swap specific shippers.

This examination is also advantageous for assessing amazing down time, i.e. how prolonged does it choose the shipper to awesome down soon after you load the dry ice? Subsequent the loading of the payload into the shipper, one particular can be expecting that there will be a awesome down time wherever the merchandise temperature will exceed the allowable storage and shipping and delivery temperature. Irrespective of whether or not this is satisfactory depends on your balance knowledge, therefore why balance details is a predecessor to performing transport qualification.

Great down time is vital data to include things like in the qualification, and it’s significant to the consumer. He shared an example showing that a shipper took around two several hours to arrive at -40°C. “The person, for illustration, loaded the shipper in the morning at 8am. And the query is ‘When can I load the product or service?’ This tells you your spec. You load it, you wait two hrs. From 10am up to 2pm is your window of prospect. You would qualify for the worst situation which would be a six-hour hold off before loading the product or service,” he stated. “Inevitably you get the query, ‘Can I use it the following day because we didn’t get to load it currently?’ My respond to is ‘No.’ The motive being that you happen to be then sacrificing shipper duration. You happen to be shedding what we are placing out to reach: highest length. So my response is to begin all around. Vacant it out and load the dry ice all over again the next working day.”

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